Carbon Nano-fragments and Nickel Glass Carbon Electrode for the Electrochemical Detection of Nifedipine

LIU Lingyu; ZHANG Yuxiang; ZHOU Fengchen; MA Zhen; YAO Chuan; ZHAO Wenbo; WU Yuhao; YE Zixing; TIE Shaolong; NAN Junmin

doi:10.6054/j.jscnun.2023019

Journal of South China Normal University (Natural Science Edition) > 2023 > 55(2): 49-54. > DOI: 10.6054/j.jscnun.2023019

LIU Lingyu, ZHANG Yuxiang, ZHOU Fengchen, MA Zhen, YAO Chuan, ZHAO Wenbo, WU Yuhao, YE Zixing, TIE Shaolong, NAN Junmin. Carbon Nano-fragments and Nickel Glass Carbon Electrode for the Electrochemical Detection of Nifedipine[J]. Journal of South China Normal University (Natural Science Edition), 2023, 55(2): 49-54. DOI: 10.6054/j.jscnun.2023019

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Carbon Nano-fragments and Nickel Glass Carbon Electrode for the Electrochemical Detection of Nifedipine

1.
Key Laboratory of Micro-Nano Materials for Energy Storage and Conversion of Henan Province, Institute of Surface Micro and Nano Materials, College of Chemical and Materials Engineering, Xuchang University, Xuchang 461000, China
2.
School of Chemistry, South China Normal University, Guangzhou 510006, China

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Received Date: March 16, 2022
Available Online: June 13, 2023

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Abstract

Abstract

Carbon nano-fragments-nickel (CNF-Ni) composites were synthesized by sol-gel thermal reduction method for the modification of glassy carbon electrodes and applied in the electrochemical sensor construction of nifedipine. The morphology and catalytic characteristic of CNF-Ni/GCE electrode were studied employing field emission scanning electron microscope, X-ray diffraction, fourier infrared spectrometer, and electrochemical technology. The results indicated that CNF-Ni/GCE electrode exhibited favourable electrocatalytic performance for nifedipine determination. Under the optimal conditions, using differential pulse voltammetry (DPV), the linear relationship between anode peak current and nifedipine concentrations was obtained from 4 to 160 μmol/L, and the detection limits was 2 μmol/L. The proposed method was employed to determine nifedipine in the actual drug detection.
- carbon nano-fragments-nickel composites,
- sol-gel thermal reduction method,
- electrochemical detection,
- nifedipine

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Carbon Nano-fragments and Nickel Glass Carbon Electrode for the Electrochemical Detection of Nifedipine

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