罗年华, 蒋飞, 韩淑娟, 黄伟聪, 朱士正, 蒋腊生. 新型功能化桥链双冠醚的合成及其结构表征[J]. 华南师范大学学报（自然科学版）, 2009, 1(4).
引用本文: 罗年华, 蒋飞, 韩淑娟, 黄伟聪, 朱士正, 蒋腊生. 新型功能化桥链双冠醚的合成及其结构表征[J]. 华南师范大学学报（自然科学版）, 2009, 1(4).
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LUO Nian-Hua, Fei JIANG, Shu-Juan HAN, Wei-Cong HUANG, Shi-ZZheng zZHU, La-Sheng JIANG. Synthesis and Characterization of novel biscrown Ethers with functionalized bridge[J]. Journal of South China Normal University (Natural Science Edition), 2009, 1(4).
Citation: LUO Nian-Hua, Fei JIANG, Shu-Juan HAN, Wei-Cong HUANG, Shi-ZZheng zZHU, La-Sheng JIANG. Synthesis and Characterization of novel biscrown Ethers with functionalized bridge[J]. Journal of South China Normal University (Natural Science Edition), 2009, 1(4).
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新型功能化桥链双冠醚的合成及其结构表征

Synthesis and Characterization of novel biscrown Ethers with functionalized bridge

    摘要
  • 摘要: 由侧链为醛基的24-冠-8和侧链为酯基的34-冠-10出发，分别经3步反应，高产率地合成了2个新型功能化桥链双冠醚4(70%)和8(71%)，并用1HNMR、13C NMR、ESI-MS等手段对这2个新型功能化桥链双冠醚4和8进行了结构表征.

     

    Abstract: Two Characterizations of novel biscrown ethers 4 and 8 were synthesized starting from 24-crown-8 with a aldehyde side arm and 34-crown-10 with a ester side arm in high yield(70% and 71%), and their structure were confirmed by 1HNMR、13C NMR、ESI-MS etc.

     

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